- BRUKER APEX II CCD DETECTOR TEST PDF
- BRUKER APEX II CCD DETECTOR TEST GENERATOR
- BRUKER APEX II CCD DETECTOR TEST UPGRADE
You no longer need a liquid chiller, so mechanical stress is reduced. NMHU X-ray Diffraction Laboratory is equipped with Bruker X-ray diffractometer SMART APEX II with CCD detector and low-temperature device that allows.
![bruker apex ii ccd detector test bruker apex ii ccd detector test](https://d12oja0ew7x0i8.cloudfront.net/images/equipments/EquipmentThumbImage_5671.jpg)
The new detector is completely air-cooled. Lysozyme diffraction image, demonstrating the high spatial resolution and sensitivity of the PHOTON II. This delivers the highest sensitivity and minimises parallax, giving you the performance necessary for weak intensities. The unique design of the PHOTON II 7 CPAD detector features an embedded scintillator, optimised for home laboratory wavelengths. Data is collected more efficiently – ideal for shared facilities and service crystallography labs. With a single monolithic sensor, there are no gaps or dead spaces between modules. Data collection is faster, with higher redundancy data for higher quality structures. This enables you to detect far more reflections in each frame. Diffractometers are: Brukar Smart Apex II (CCD) Bruker D8 VENTURE (CMOS photon 100). An even larger area is available with the PHOTON II 14 (10 cm x 14 cm). Which detector (CCD vs CMOS) should give better quality of data.
![bruker apex ii ccd detector test bruker apex ii ccd detector test](https://kuleuven.xct.be/wp-content/uploads/2021/03/InSituInfusion1.png)
The PHOTON II 7 detector has an active area of 70 cm², which is almost twice the size of the previous APEX II. Shutterless mode enables you to acquire data faster, with a higher level of quality. This eliminates overhead time and mechanical jitter, which can be a problem with stop-start shuttered-mode operation. Data is collected while the sample rotates continuously. Cell refinement and data reduction were managed by CrysAlisPro (Agilent Technologies). Shutterless mode gives you better data, in a faster timeframe. The intensity data for these compounds were generated at 293.58 K on a Bruker APEX-II CCD detector employing graphite monochromated Cu-K radiation ( 1.54178 ). There are two models offering a choice of sizes. Such a comparison is especially valuable since the data had been measured using a well established methodology applying a Bruker AXS CCD-type APEX II detector at a synchrotron beamline known for accurate and precise electron density studies.
BRUKER APEX II CCD DETECTOR TEST UPGRADE
We’re available to advise about upgrade compatiblity, so if you have any questions please get in touch.įor SMART APEX and KAPPA APEX owners, if you decide to upgrade later to a D8 QUEST or D8 VENTURE, the PHOTON II detector can be transferred to your new instrument, reducing the cost in future. The Bruker PHOTON II is available for these SC-XRD systems, both with new instruments and as an upgrade: Semiempirical multi-scan absorption corrections were applied by using SADABS. Instrument is equipped with a Moly rotating anode source and a Photon III detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-500 K.3D diffraction image of a transition metal complex (3 seconds exposure). Diffraction intensities of 1 were collected on a Bruker APEX-II CCD diffractometer equipped with a graphite-monochromatic Mo K radiation with a radiation wavelength of 0.71073 by using the scan technique at 296 K. Instrument is equipped with a Gallium MetalJet source and a Photon III detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-500 K.
![bruker apex ii ccd detector test bruker apex ii ccd detector test](https://www.sheffield.ac.uk/sites/default/files/styles/mobile_single_column_1x/public/2020-01/IMG_5271.JPG.jpg)
The only difference is the thickness of the scintillation phosphor, which results in a characteristic quantumyield of 160 eperX-rayphoton forMo K and 204 e per X-ray photon for Ag K.
BRUKER APEX II CCD DETECTOR TEST GENERATOR
It is equipped with a Copper MicroMax 003f X-ray generator and PILATUS R200K Hybrid Pixel Array Detector as well as an Oxford Cryosystems Cobra for variable temperature data collection from 90-400 K.īruker D8 Venture Diffractometer-Ga MetalJet with Bruker APEX II area detectors that use Fairchild CCD6161 sensors. Data were collected in 0.5 oscillations with 10 second exposures. The data were collected at a temperature of 100(2) K with a theta range for data collection of 1.37 to 26.31. Instrument is currently located on the BioSide of campus. made on a Bruker APEX-II CCD diffractometer with graphite monochromated Mo-K radiation. APEX II CCD Diffractometer December 9th, 2016 Matthias Zeller Purdue University, West Lafayette, PA, 47907, USA The following is guide for collecting data and solving structures using a Bruker APEX II single crystal diffractometer.
BRUKER APEX II CCD DETECTOR TEST PDF
usable angular range: 30 to 1350 Diffrac plus software Wavelength: 1.5406 A0 PDF 2 and Topaz P available Lynx Eye Detector Low/ High Temp. X-Ray Diffractometer (Powder) Bruker AXS D8 Advance Max. Dual source instrument equipped with a TRIUMPH monochromated Moly sealed tube and a Copper IµS. System features a Kappa goniometer and a Photon II detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-400 K. Bruker AXS Kappa APEX II CCD KAPPA 4 Axis Goniometer KRYO-FLEX Low Temp Device Structure Elucidation Software SHELXTL Single crystal structure analysis 3.